1D 1H, 13C, 31P, 19F spectra
1D 1H selective decoupling data
Variable temperature data, from 5°C to 130°C
2D 1H-1H COSY, 1H-1H NOESY, 1H-1H TOCSY
2D 1H-13C HSQC, 1H-13C HMBC
With longer turn-around time, we conduct research level data acquisition
1D spectra of 11B, 29Si, 23Na, or any other NMR active nuclei
NMR data sets of very limited quantity material (HMBC data with 20 µg of compound with M.W. about 500)
2D or 3D solution NMR data sets of proteins
Solid state NMR data
We will also provide data analysis upon request. For example, spectral assignment, J-coupling constant calculation, stereochemistry determination.
Instruments used: Bruker 400MHz AVANCE, Varian 400MHz and Varian 500 Unity Inova. Usage of 600MHz or 750MHz instrument can be arranged when there is a need for it.
Various ligand-protein binding study data, such as STD, waterLOGSY
We routinely acquire NMR data that a chemist typically needs. They include, but are not limited to
Data analysis, e.g. spectral assignment, J-coupling constant calculation, conformation determination
Water or multiple solvent suppression 1H data
Data of other NMR active nuclei, e.g. 29Si, 11B, 195Pt
1H – 13C 2D HSQC data
1H – 13C 2D long range correlation experiment HMBC data
Variable temperature NMR, range: 5°C to 130°C
13C DEPT data
1H – 1H 2D COSY, NOESY or TOCSY data
1D NOE or 1H with selective decoupling data
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